Distillation

Distillation: Fundamentals and Principles — winner of the 2015 PROSE Award in Chemistry & Physics — is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on the conceptual design of distillation. Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers Practical information on the newest development written by recognized experts Coverage of a huge range of laboratory and industrial distillation approaches Extensive references for each chapter facilitates further study

This work contains the proceedings of the Distillation and Absorption conference, which happens every 5 years. This collection of 100 contributions spanning 23 countries showcase the newest and best distillation and absorption technologies which cover a broad range of fundamental and applied aspects of the technology. To address these aspects, the contributions have been put into seven themes: modelling and simulation (steady-state, dynamic and CFD); energy efficiency and sustainability; equipment design and operation; integrated, hybrid and novel processes; process troubleshooting and handling operational problems; control and operation; and basic data.

Originally published in 2004, Distillation Theory and Its Application to Optimal Design of Separation Units presents a clear, multidimensional geometric representation of distillation theory that is valid for all distillation column types, splits, and mixtures. This representation answers such fundamental questions as: what are the feasible separation products for a given mixture? What minimum power is required to separate a given mixture? What minimum number of trays is necessary to separate a given mixture at a fixed power input? This book is intended for students and specialists in the design and operation of separation units in the chemical, pharmaceutical, food, wood, petrochemical, oil-refining, and natural gas industries and for software designers.

While most wine and spirits books focus on vineyard and crop management or fermentation and distillation processes, few address critical post process aspects of stabilization, aging, and spoilage. This book serves as a comprehensive source of information on post-fermentation and -distillation technology applied to wine, beer, vinegar and distillates in a broad spectrum. Post-Fermentation and -Distillation Technology: Stabilization, Aging, and Spoilage thoroughly describes all of the operations related to these products after the fermentation or distillation steps, focusing on the complex issues related to their stabilization, aging, and spoilage. The final product must be stable against microbial activity as well as undesirable chemical and physical chemical reactions that occur in the bottle. For example, clarity, stability, compositional adjustment, style development and packaging represent the five goals of "finishing" a wine. Concerning the visual defects associated with spoilage, it is crucial that wine at the point of consumption not be cloudy or contain any haze or precipitate, especially white wines. Similarly, it is also important to prevent unwanted microbial growth from occurring in the wine after the primary fermentation is complete, affecting the flavor and aroma profile in unpredicted ways. The book addresses all of these issues and more. Moreover, the discussion also involves beer, vinegar and distillates, giving this book a novel and interesting approach. The book combines referenced research with practical applications and case studies of novel technologies such as square barrels, synthetic closures, and Tetra Pak®.

Hardbound. In addition to the three main themes: chemical reactors, distillation columns, and batch processes this volume also addresses some of the new trends in dynamics and control methodology such as model based predictive control, new methods for identification of dynamic models, nonlinear control theory and the application of neural networks to identification and control. Provides a useful reference source of the major advances in the field.

Distillation Principles and Practice Second Edition covers all the main aspects of distillation including the thermodynamics of vapor/liquid equilibrium, the principles of distillation, the synthesis of distillation processes, the design of the equipment, and the control of process operation. Most textbooks deal in detail with the principles and laws of distilling binary mixtures. When it comes to multi-component mixtures, they refer to computer software nowadays available. One of the special features of the second edition is a clear and easy understandable presentation of the principles and laws of ternary distillation. The right understanding of ternary distillation is the link to a better understanding of multi-component distillation. Ternary distillation is the basis for a conceptual process design, for separating azeotropic mixtures by using an entrainer, and for reactive distillation, which is a rapidly developing field of distillation. Another special feature of the book is the design of distillation equipment, i.e. tray columns and packed columns. In practice, empirical know-how is preferably used in many companies, often in form of empirical equations, which are not even dimensionally correct. The objective of the proposed book is the derivation of the relevant equations for column design based on first principles. The field of column design is permanently developing with respect to the type of equipment used and the know-how of two-phase flow and interfacial mass transfer.

The Art of Distilling, Revised and Expanded presents the techniques and inspirations of the most innovative micro-distillers working today and ties it together with incredible insider photography. In this comprehensive guide to artisan distilling, American Distilling Institute founder Bill Owens will teach you how contemporary master distillers transform water and grain into the full range of exquisite, timeless spirits. The Art of Distilling, Revised and Expanded is your exclusive backstage pass into the world of small-scale distilling of whiskies, gins, vodkas, brandies, and many other spirits. Like no other book on the subject, The Art of Distilling goes to lengths to explore the actual craft of distilling, in detail. Beginning with a brief history of distilling and introduction to the process itself, this book offers a comprehensive overview of the art of distilling today. The revised and expanded edition includes even more practical tips, tricks, and instruction and has been updated to include growth and development in the artisan distilling space over the past decade. The Art of Distilling, Revised and Expanded is the consummate insider's guide to distilling and its techniques.

Modern membrane engineering is critical to the development of process-intensification strategies and to the stimulation of industrial growth. Membrane Distillation (MD) is a broad reference that covers specific information on membranes available and methods for MD membrane preparation and characterization. The book offers an introduction to the terminology and fundamental concepts as well as a historical review of MD development. Commercial membranes used in MD as well as laboratory-made membranes, including emerging membranes, are described in detail and illustrated by a number of clear and instructive schematic drawings and images. A comprehensive review on the development of MD membranes, MD modules, MD membrane characterization, MD configurations, applications in different areas and theoretical models Introduction to the terminology and fundamental concepts associated with MD as well as an historical review of MD development Description of commercial membranes used in MD as well as laboratory-made membranes, including emerging membranes

The complete guide for beginner and intermediate distillers. Make your own brew at home! ”If you’re going to invest the $100 or so to get a basic equipment and recipe kit, then you’ll want to take care in ensuring that your first batch is brewed correctly.” –Rick Morris, HowBrewBeer The Joy of Home Distilling is covers nearly every facet of distilling: Step-by-step instructions for the different processes, from bucket to bottle The difference between spirit types and how to produce each What yeast is, what it does, and how to ensure that you get a strong, complete fermentation What distillation is and common misconceptions about the process Legalities surrounding distilling alcohol at home Carbon filtering—when it’s necessary, when to filter, and why you filter Flavoring and aging your spirits Keeping safety first when working with flammable materials, such as ethanol Yeast styles and nutritional requirements Different methods of distillation and equipment Post-distillation process And of course, fun drink recipes! (Try the Mudslide or the Cherry Bomb!) Author Rick Morris, who has been selling distillation equipment for over 25 years, even includes his own recipes for different types of spirits and drink recipes. By learning not just how to distill, but also what is happening at each step and why it is needed, readers will be armed with the information they need to experiment with their own spirits and concoct their own recipes. Easy to understand even for a first-time distiller, The Joy of Home Distilling is sure to become your number one distilling resource.

Special Distillation Processes, Second Edition focuses on the latest developments in the field, such as separation methods that may prove useful for solving problems encountered during research. Topics include extraction, membrane and adsorption distillation involving the separation principle, process design and experimental techniques. The relationship between processes and techniques are also presented. Comprehensive and easy-to-read, this book provides key information needed to understand processes. It will be a valuable reference source for chemical engineers and students wishing to branch out in chemical engineering. Provides the only comprehensive book available on special distillation processes Contains a thorough introduction to recent developments in the field Presents a valuable reference for students, academics and engineers in chemical engineering